专利名称 | Herstellung von einwandigen Kohlenstoffnanor?hren | 申请号 | DE20006028869T | 专利类型 | DE | 公开(公告)号 | DE60028869(T2) | 公开(授权)日 | 2007.01.18 | 申请(专利权)人 | 中国科学院金属研究所 | 发明(设计)人 | CHENG HUIMING (CN);LIU CHANG (CN);CONG HONGTAO (CN);LIU MIN (CN);FAN YUEYING (CN);SU GE (CN) | 主分类号 | C01B31/00 | IPC主分类号 | C01B31/00;C01B31/02;B01J19/08;C01B3/00;D01F9/1220060101C;D01F9/1220060101A | 专利有效期 | Herstellung von einwandigen Kohlenstoffnanor?hren 至Herstellung von einwandigen Kohlenstoffnanor?hren | 法律状态 | 说明书摘要 |
The present invention relates to a large-scale hydrogen arc discharge method for the synthesis of single-walled carbon nanotubes (SWNTs): Under the atmosphere of H2, a large-size anode composed of graphite powders, catalyst metals and growth promoter is consumed with the growth of SWNTs; The angle between the anode and cathode can be adjusted in the range of 30 DEG -80 DEG ; The catalysts used can be two or more kinds of metals selected from Fe, Co, Ni and Y, which have been proved to be essential for the growth of SWNTs; The proportion of catalysts is modified in the range of 2.5-5.0 at%. By these processes, large-scale SWNTs can be synthesized with the advantages of semi-continuous synthesis, low cost and high quality, and the SWNTs obtained can be then employed as a kind of promising hydrogen storage material. |
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