Low molecular weight chitosan oligosaccharides and its preparation method

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专利名称 Low molecular weight chitosan oligosaccharides and its preparation method 申请号 US20030560296 专利类型 US 公开(公告)号 US2007089978 公开(授权)日 2007.04.26 申请(专利权)人 中国科学院海洋研究所 发明(设计)人 LI PENGCHENG (CN);XING RONGE (CN);LIU SONG (CN);YU HUAHUA (CN) 主分类号 C08B37/08 IPC主分类号 C08B37/08;C08B37/00 专利有效期 Low molecular weight chitosan oligosaccharides and its preparation method 至Low molecular weight chitosan oligosaccharides and its preparation method 法律状态 说明书摘要 The present invention relates to low molecular weight chitosan oligosaccharides and its preparation method. Chitosan oligosaccharides were obtained under microwave irradiation assisted the electrolyte. The method of preparing chitosan oligosaccharides was described as follows: acid solvent containing electrolyte was added to chitosan. The reaction was performed at 480~800 W for 3~12 min. After irradiation ceased, the reaction liquid was cooled to room temperature. Then the solution was adjusted to neutrality with 1~10 M NaOH or KOH and obtained the pale yellow floc. The processes of precipitation, filtering, desiccation and crushing are settled sequentially. Finally, chitosan oligosaccharides were obtained. Method of the present invention makes chitosan degrade to water-soluble chitosan oligosaccharides and it makes some inert substance become active. The method of the present invention can cut down energy consumption, decrease pollution and save time and raw materials. It has applying perspective of industry and potentiality of extensive market.

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